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University of Limerick, Bernal Institute, Limerick, V94 T9PX

SEM Raman

InVia Raman confocal spectrometer offers spectral, depth profiling and mapping acquisitions to provide high resolution chemical and molecular information on a wide variety of sample types.

SEMRenishaw InVia Raman spectrophotometer

SEM-Raman interfacing (SEM-SCA) enables simultaneous chemical characterisation coupled with high resolution imaging of organic nanostructures. JSM-6510 SEM operates in low and high-vacuum modes to facilitate the investigation of uncoated non- conducting samples.
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Renishaw InVia Raman spectrophotometer specifications

  • Dual excitation sources (532 nm and 785 nm lasers)
  • An optical microscope (Leica) with high quality objective lenses
  • A motorised spectrometer lenses which automatically align for each configuration
  • Grating stage with dual gratings (1800 lines mm-1 for 532 nm and 1200 lines mm-1 for 785 nm)
  • A thermoelectrically cooled (- 70 ºC) CCD detector
  • Spot size of < 2 μm for 50x objective lens
  • Spatial resolution < 1 μm
  • Laser line specific Rayleigh filters with a dual filter arrangement to optimise sensitivity
  • Raman shift range of 100 – 4000 cm−1
  • A Raman   probe   and   SEM   interface   for   coupling   the   InVia spectrophotometer to an SEM
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JSM-6510LV Scanning Electron Microscope specifications

  • Operating voltage of 1-30 kV.
  • Resolution: High-vacuum mode:
      • 30 kV 0 nm (SEI, 8 mm WD)
      • 3 kV 8.0 nm (SEI, 6 mm WD)
      • 1 kV 15 nm (SEI, 6 mm WD)
  • Magnification of 5x – 300, 000x
  • Pressure range in the specimen chamber: 10 to 270 Pa
  • Image Signals:
      • High-vacuum mode: secondary electron and backscattered electron imaging
      • Low-vacuum mode: backscattered electron imaging, Multi- element solid state BSE detector standard on LV models
  • Working distances 5-40 mm with tilt -5 – 70 degrees
  • BSE Detector with 3 nm resolution
  • Stage navigation system